HRID1634896

反应详情

EQUATION

反应方程式

HRID 1634896 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Ethyl 3-[2-(3,4,5-trimethoxyphenyl)pyridin-4-yl]propenoate (579 mg) was dissolved in methanol (20 mL), 10% palladium on carbon (60 mg) was added to the solution, and the mixture was stirred at room temperature for 6 hours under a hydrogen atmosphere. The catalyst was removed by filtration, and the filtrate was concentrated under reduced pressure to obtain the title compound.

WORKUP

后处理

  1. customThe catalyst was removed by filtration
  2. concentrationthe filtrate was concentrated under reduced pressure