HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69529373, compound → Ethyl 3-[2-(3,4,5-trimethoxyphenyl)pyridin-4-yl]propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69529373 | HCID 69529373 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl 3-[2-(3,4,5-trimethoxyphenyl)pyridin-4-yl]propionate | HCID 18674991 | — |
Reaction Steps
Ethyl 3-[2-(3,4,5-trimethoxyphenyl)pyridin-4-yl]propenoate (579 mg) was dissolved in methanol (20 mL), 10% palladium on carbon (60 mg) was added to the solution, and the mixture was stirred at room temperature for 6 hours under a hydrogen atmosphere. The catalyst was removed by filtration, and the filtrate was concentrated under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509329B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-0d0e6ebaa2d04065920da8266718c08b |
| Source note | uspto-grants-2003_01 |