HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18676179, compound → HCID 18676177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18676179 | HCID 18676179 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 18676177 | HCID 18676177 | 101.5% |
Reaction Steps
A solution of 58 mg of {2-[(2-{[(2-chloro-3,4-dimethoxyphenyl)-N-(3-methylbutyl)carbonylamino]methyl}-4,5-dimethylimidazol-1-yl)methyl]phenoxy}acetate in 2 mL of 5N HCl is heated under reflux for 15 min. The volatiles are evaporated under reduced pressure, and the residue is dried in a vacuum oven at 90° C. to give 59 mg of the title compound as the hydrochloride salt. Mass Spec m/z (M++1) 558.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509366B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-2f8e4a8c22f04624b29b0781ec01b2d0 |
| Source note | uspto-grants-2003_01 |