HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 12468339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 622378 | HCID 622378 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 12468339 | HCID 12468339 | 93% |
Reaction Steps
To a stirred solution of 1-phenyl-6,7-dimethoxy-3,4-dihydroisoquinoline in acetone was added methyl iodide and the reaction mixture was stirred at room temperature for 16 hours. A pale yellow precipitate was formed. The by-products and unreacted methyl iodide were removed in vacuo to afford the desired compound in 93% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509467B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-b1c7ba3e56924271bdd4be34b654d294 |
| Source note | uspto-grants-2003_01 |