Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1635774Generated: October 26, 2026

2-Tridecyn-1-ol → 1-Bromo-2-tridecyne

https://huagongshe.com/reaction/1635774

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Tridecyn-1-olHCID 11116979—
ReactantCBr4 triphenylphosphineHCID 11387777—
SolventDichloromethaneHCID 6344—
Product1-Bromo-2-tridecyneHCID 18673385—

Reaction Steps

1-Bromo-2-tridecyne (colorless oil) was prepared from 2-tridecyn-1-ol using the CBr4/triphenylphosphine mixture in dichloromethane to carry out the halogenation. 1-Bromo-2-tridecyne (colorless oil) was thus formed with a yield of 91%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06511670B1
Source datasetuspto-grants-2003_01
ORD IDord-ed1dc395dd2147808413d595d6032b70
Source noteuspto-grants-2003_01