Sodium Iodide → HCID 22719916, compound

HRID 1635911Notes

Reaction equation

HRID 1635911 reaction equation
F[P-](F)(F)(F)(F)F.[CH3:8][N+:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][C:16]([C:18]1[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=1)=[O:17].[Na+].[I-:26]>CC(C)=O>[I-:26].[CH3:8][N+:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][C:16]([C:18]1[CH:19]=[CH:20][C:21]([CH3:24])=[CH:22][CH:23]=1)=[O:17]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 15487510HCID 15487510, compound

Product 1

HCID 22719916HCID 22719916, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

10 mmol of the compound obtained in Example 1 are dissolved in 35 ml of acetone, and 15 mmol of NaI are added in portions of 100 mg. A white precipitate is obtained immediately and the mixture is stirred for 14 hours in a sealed tube at ambient temperature. The white solid obtained is filtered off and washed with acetone.

Workup

  1. customA white precipitate is obtained immediately
  2. customThe white solid obtained
  3. filtrationis filtered off
  4. washwashed with acetone

Sources & evidence

ORD record
ord-da2dca5238dd48f7bf661a2c674bea31
Source dataset
uspto-grants-2003_01
Patent number
US06511992B2

Reaction notes

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