HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-(9H-carbazol-2-yloxy)-octanoic acid benzyloxyamide → HCID 9967789, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-(9H-carbazol-2-yloxy)-octanoic acid benzyloxyamide | HCID 86586543 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9967789 | HCID 9967789 | 0% |
Reaction Steps
In a manner anologous to that of example 1(c), 8-(9H-carbazol-2-yloxy)-octanoic acid benzyloxyamide (90 mg, 430 mmol) in tetrahydrofuran was hydrogenated in the presence of palladium on barium sulfate to give the title compound as a crystalline solid (16 mg). MS (M−H+)=339.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06512123B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-3baacf172d4b45bfbb116e363b726e64 |
| Source note | uspto-grants-2003_01 |