HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 17770918, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2,4,5-Trifluoro-3-(trifluoromethyl)benzoic acid | HCID 14278827 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 17770918 | HCID 17770918 | — |
Reaction Steps
30 ml of benzene, 17 ml of thionyl chloride and several drops of N,N-dimethylformamide were added to 8.5 g (0.0348 mole) of 2,4,5-trifluoro-3-trifluoromethylbenzoic acid (VII), and the mixture was refluxed under heating for 3 hours. After the reaction, benzene and excess thionyl chloride were removed by evaporation under reduced pressure to obtain 2,4,5-trifluoro-3-trifluoromethylbenzoic acid chloride (VIII).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034086 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-5555a0aac2d74b81ac5acd052400a5bd |
| Source note | uspto-grants-2000_03 |