HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 19350832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 54154960 | HCID 54154960 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19350832 | HCID 19350832 | — |
Reaction Steps
1-(5-Benzyloxymethyl-1,4-oxathian-2-yl)-N4 -acetylcytosine (0.31 g) was dissolved in methanol (10 ml), and 0.43M sodium methoxide solution (1 ml) was added to the solution. The resultant mixture was stirred at room temperature for one hour to complete the reaction. The reaction mixture was neutralized with acetic acid, and the solvent was removed by evaporation under reduced pressure to obtain pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034087 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-ddf0298f547a43dbac15bfc46c7a9cb3 |
| Source note | uspto-grants-2000_03 |