Diethylamine → HCID 178440312, compound

HRID 1636353Notes

Reaction equation

[CH2:1]([C:3]1[CH:28]=[CH:27][CH:26]=[CH:25][C:4]=1[NH:5][CH:6]=[C:7]1[C:11](=[O:12])[N:10]([C:13]2[CH:21]=[CH:20][C:16]([C:17](O)=[O:18])=[CH:15][CH:14]=2)[N:9]=[C:8]1[CH2:22][CH2:23][CH3:24])[CH3:2].[CH2:29]([NH:31][CH2:32][CH3:33])[CH3:30]>>[CH2:29]([N:31]([CH2:32][CH3:33])[C:17](=[O:18])[C:16]1[CH:20]=[CH:21][C:13]([N:10]2[C:11](=[O:12])[C:7](=[CH:6][NH:5][C:4]3[CH:25]=[CH:26][CH:27]=[CH:28][C:3]=3[CH2:1][CH3:2])[C:8]([CH2:22][CH2:23][CH3:24])=[N:9]2)=[CH:14][CH:15]=1)[CH3:30]

Participants

Reactant 2

HCID 8021Diethylamine

HCID 178440313HCID 178440313, compound

Product 1

HCID 178440312HCID 178440312, compound

Procedure

From the reaction of 4-(4-(2-ethylanilinomethylene)-4,5-dihydro-5-oxo-3-propyl-1H-pyrazol-1-yl)-benzoic acid and diluted diethylamine solution, N,N-diethyl-4-(4-(2-ethylanilinomethylene)-4,5-dihydro-5-oxo-3-propyl-1H-pyrazol-1-yl)-benzamide is obtained, Mp 123° C.

Sources & evidence

ORD record: ord-943d9693887e4e2d9216d7a9fc0380d7
Source dataset: uspto-grants-2000_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06034099

Reaction notes

Loading…