Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | 2-Methylidenedodecanamide | HCID 21275879 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | n-Decylacrylamide Acrylamid | HCID 21275878 | — |
Reaction Steps
To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux condenser, and septum was added 150 mL of isopropanol followed by 16.13 g of a 50% aqueous solution of 2-trimethylammoniumethylacrylate chloride, 8.06 g of n-decylacrylamide, and 8.06 g of acrylamide. The solution was purged with nitrogen for 1 hour and 0.5 g AIBN was added. The mixture was purged for -15 minutes until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06034129 |
|---|
| Source dataset | uspto-grants-2000_03 |
|---|
| ORD ID | ord-cfaf9d45407542109e78203782f6f65e |
|---|
| Source note | uspto-grants-2000_03 |
|---|