HRID1636465

反应详情

EQUATION

反应方程式

HRID 1636465 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 10.0 g (58 mmol) 1-methoxycarbonyl-2-vinylcyclopropane carboxylic acid, 14.0 g trimethoxysilylpropylglycidyl-ether and 100 mg lithium perchlorate in 20 ml dichloromethane were stirred at room temperature for 15 days. After removal of solvent in vacuo, 20 g (83% yield) of a clear, yellow viscous liquid remained.

WORKUP

后处理

  1. customAfter removal of solvent in vacuo, 20 g (83% yield) of a clear, yellow viscous liquid