HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 19352176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Benzenamine, 4-(2-benzoxazolyl)- | HCID 88733 | — |
| Reactant | HCID 385071 | HCID 385071 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 19352176 | HCID 19352176 | — |
Reaction Steps
2-(4'-Aminophenyl)benzoxazole (0.28 g, 1.33 mmol) was treated with chloroacetyl chloride (0.5 ml) in benzene (15 ml) according to the procedure described above for preparation of 2-(4'-chloroacetamidophenyl)benzothiazole. 2-(4'-Chloroacetamidophenyl)benzoxazole hydrochloride was obtained (0.31 g, 72%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034246 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-65420691235d4d3f95025ab355bdcbe8 |
| Source note | uspto-grants-2000_03 |