HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylallylamine → HCID 18434343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylallylamine | HCID 69391 | — |
| Reactant | 6-Bromo-1-hexanol | HCID 77970 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 18434343 | HCID 18434343 | — |
Reaction Steps
1 ml of 1-bromo-6-hexanol are taken up in DMA, treated with 1.47 ml of N-allyl-methyl-amine and stirred at RT for 16 h. The reaction mixture is concentrated and the residue is lyophilized overnight. There are obtained 1.9 g of 6-(allyl-methyl-amino)-hexan-1-ol.hydrobromide as the crude product, MS: m/e 171 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034275 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-159fbc93d702465b8b7c682573def035 |
| Source note | uspto-grants-2000_03 |