N-Methylallylamine → HCID 18434343, compound

HRID 1636755Notes

Reaction equation

HRID 1636755 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][OH:8].[CH2:9]([NH:12][CH3:13])[CH:10]=[CH2:11]>CC(N(C)C)=O>[BrH:1].[CH2:9]([N:12]([CH3:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][OH:8])[CH:10]=[CH2:11]

Participants

4

Reactant 2

HCID 69391N-MethylallylamineHCID 779706-Bromo-1-hexanol

Product 1

HCID 18434343HCID 18434343, compound

Reagents, catalysts & solvents 1

HCID 31374DimethylacetamideSolvent

Procedure

1 ml of 1-bromo-6-hexanol are taken up in DMA, treated with 1.47 ml of N-allyl-methyl-amine and stirred at RT for 16 h. The reaction mixture is concentrated and the residue is lyophilized overnight. There are obtained 1.9 g of 6-(allyl-methyl-amino)-hexan-1-ol.hydrobromide as the crude product, MS: m/e 171 (M).

Workup

  1. concentrationThe reaction mixture is concentrated
  2. waitthe residue is lyophilized overnight

Sources & evidence

ORD record
ord-159fbc93d702465b8b7c682573def035
Source dataset
uspto-grants-2000_03
Patent number
US06034275

Reaction notes

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