HCID 19349789, compound → HCID 19349785, compound

Participants

Reaction Steps

The nitro group is reduced as follows: To a 250 ml Parr bottle are added 800 mg (3.9 mmol) of 3-(1-methyltetrazol-3-yl)nitrobenzene, 200 mg platinum oxide, and 75 ml ethanol. The reaction is pressurized with 45 p.s.i. hydrogen for 1 hour, then catalyst removed by filtration, and the solvent evaporated to afford 635 mg (93.0%) of a white solid, mp 93°-95° C.

Provenance & Evidence