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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1637011Generated: November 2, 2026

HCID 53837207, compound → 2-(2-hydroxymethylphenyl)-2-methoxyimino-N-methylacetamide

https://huagongshe.com/reaction/1637011

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53837207HCID 53837207—
ReactantMonomethylamine methanolHCID 57454252—
SolventMethanolHCID 887—
Product2-(2-hydroxymethylphenyl)-2-methoxyimino-N-methylacetamideHCID 54472560—

Reaction Steps

A mixture of 2-(2-acetoxymethylphenyl)-2-methoxyiminoacetamide (194 mg, E/Z≠79/21), methanol (3.0 ml) and a 40% methylamine/methanol solution (1.0 ml) was stirred at 40° C. for 3 hours. After the mixture was ice-cooled, the solvent was evaporated under reduced pressure to obtain the crude product (203 mg, E/Z≠91/9) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06037495
Source datasetuspto-grants-2000_03
ORD IDord-ebcb612826b64e44832bab593028e4f1
Source noteuspto-grants-2000_03