HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53837207, compound → 2-(2-hydroxymethylphenyl)-2-methoxyimino-N-methylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53837207 | HCID 53837207 | — |
| Reactant | Monomethylamine methanol | HCID 57454252 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(2-hydroxymethylphenyl)-2-methoxyimino-N-methylacetamide | HCID 54472560 | — |
Reaction Steps
A mixture of 2-(2-acetoxymethylphenyl)-2-methoxyiminoacetamide (194 mg, E/Z≠79/21), methanol (3.0 ml) and a 40% methylamine/methanol solution (1.0 ml) was stirred at 40° C. for 3 hours. After the mixture was ice-cooled, the solvent was evaporated under reduced pressure to obtain the crude product (203 mg, E/Z≠91/9) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06037495 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-ebcb612826b64e44832bab593028e4f1 |
| Source note | uspto-grants-2000_03 |