HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine hydrochloride → HCID 178515925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine hydrochloride | HCID 11130 | — |
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178515925 | HCID 178515925 | 83% |
Reaction Steps
Into the same device as used in Example 1 were placed 1.19 g (0.010 mole) of paracyanophenol, 1.95 g (0.030 mole) of sodium azide, 4.13 g (0.030 mole) of triethylamine hydrochloride and 12 ml of toluene. The mixture was reacted for 8 hours in the same manner as in Example 1, giving 1.34 g (0.0083 mole) of 5-(4-hydroxyphenyl)-1H-tetrazole (yield 82.7% based on paracyanophenol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06040454 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-f82a0ae4786c45b086c6e210f65f90bd |
| Source note | uspto-grants-2000_03 |