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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1637398Generated: November 1, 2026

1-Methylimidazole → HCID 86755252, compound

https://huagongshe.com/reaction/1637398

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-MethylimidazoleHCID 1390—
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 19349301HCID 19349301—
ProductHCID 86755252HCID 86755252—

Reaction Conditions

Temperature135 °C

Reaction Steps

22.5 parts of N,N-dipropoxy-m-aminophenol were charged to a reactor vessel followed by 22.0 parts of-acetic anhydride and 0.5 parts of 1-methylimidazole. The mixture was then heated to about 130 to 140° C. and held for 3 hours. The acetic acid and excess anhydride were then distilled out at a temperature from 130 to 140° C. leaving the N,N-dipropoxy-m-aminophenol diacetate product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06040482
Source datasetuspto-grants-2000_03
ORD IDord-cd8e83f54dfb4007a5fd704fcefb4373
Source noteuspto-grants-2000_03