Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Methylimidazole | HCID 1390 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 19349301 | HCID 19349301 | — |
| Product | HCID 86755252 | HCID 86755252 | — |
Reaction Steps
22.5 parts of N,N-dipropoxy-m-aminophenol were charged to a reactor vessel followed by 22.0 parts of-acetic anhydride and 0.5 parts of 1-methylimidazole. The mixture was then heated to about 130 to 140° C. and held for 3 hours. The acetic acid and excess anhydride were then distilled out at a temperature from 130 to 140° C. leaving the N,N-dipropoxy-m-aminophenol diacetate product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06040482 |
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| Source dataset | uspto-grants-2000_03 |
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| ORD ID | ord-cd8e83f54dfb4007a5fd704fcefb4373 |
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| Source note | uspto-grants-2000_03 |
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