HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isonicotinamide → N-(2-t-Butyl-5-[(4-pyridyl)carbonylaminocarbonyl]phenyl)-3-(2,4-dimethoxyphenyl)octanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isonicotinamide | HCID 15074 | — |
| Reactant | HCID 19348635 | HCID 19348635 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-(2-t-Butyl-5-[(4-pyridyl)carbonylaminocarbonyl]phenyl)-3-(2,4-dimethoxyphenyl)octanamide | HCID 19348755 | — |
Reaction Steps
Following a similar procedure to that described in Example 139, but using N-(2-t-butyl-5-carboxyphenyl)-3-(2,4-dimethoxyphenyl)octanamide (prepared as described in Preparation 7) and isonicotinamide, the title compound was obtained as crystals, melting at 184-185° C. (from ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06040339 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-40bea00369454ec09e3835b6e4a9c597 |
| Source note | uspto-grants-2000_03 |