HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyramide → Diisopropyl Ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyramide | HCID 68424 | — |
| Reactant | N-(2-t-butyl-5-carboxyphenyl)-3-(2,4-dimethoxyphenyl)heptanamide | HCID 19348750 | — |
| Product | Diisopropyl Ether | HCID 7914 | — |
| Product | N-[2-t-Butyl-5-(2-methylpropanoyl)aminocarbonylphenyl]-3-(2,4-dimethoxyphenyl)heptanamide | HCID 19348690 | — |
Reaction Steps
Following a similar procedure to that described in Example 139, but using 2-methylpropanamide and N-(2-t-butyl-5-carboxyphenyl)-3-(2,4-dimethoxyphenyl)heptanamide (prepared as described in Preparation 31B), the title compound was obtained as crystals, melting at 139-140° C. (from diisopropyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06040339 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-4a2ed6b94c9842d69d5b235abc161389 |
| Source note | uspto-grants-2000_03 |