Methylamine → HCID 19348484, compound

HRID 1637478Notes

Reaction equation

[C:1]([C:5]1[CH:10]=[CH:9][C:8]([CH2:11][CH2:12][C:13](O)=[O:14])=[CH:7][C:6]=1[NH:16][C:17](=[O:37])[CH2:18][CH:19]([C:25]1[CH:30]=[C:29]([O:31][CH3:32])[C:28]([O:33][CH3:34])=[CH:27][C:26]=1[O:35][CH3:36])[CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])([CH3:4])([CH3:3])[CH3:2].[CH3:38][NH2:39]>>[C:1]([C:5]1[CH:10]=[CH:9][C:8]([CH2:11][CH2:12][C:13]([NH:39][CH3:38])=[O:14])=[CH:7][C:6]=1[NH:16][C:17](=[O:37])[CH2:18][CH:19]([C:25]1[CH:30]=[C:29]([O:31][CH3:32])[C:28]([O:33][CH3:34])=[CH:27][C:26]=1[O:35][CH3:36])[CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 6329Methylamine

HCID 19348544HCID 19348544, compound

Product 1

HCID 19348484HCID 19348484, compound

Procedure

Following a similar procedure to that described in Example 8, but using N-[2-t-butyl-5-(2-carboxyethyl)phenyl]-3-(2,4,5-trimethoxyphenyl)octanamide (prepared as described in Preparation 84) and methylamine, the title compound was obtained as a colorless foam-like substance.

Sources & evidence

ORD record: ord-7748badb54f04ce7bd56ac69fb8454c0
Source dataset: uspto-grants-2000_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06040339

Reaction notes

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