Sodium ethoxide → HCID 19348676, compound

HRID 1637532Notes

Reaction equation

HRID 1637532 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([CH:13]([CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:14][C:15]([OH:17])=[O:16])=[C:9]([O:23][CH3:24])[CH:8]=1.[O-][CH2:26]C.[Na+].C[O-].[Na+]>>[CH2:1]([O:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([CH:13]([CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH2:14][C:15]([OH:17])=[O:16])=[C:9]([O:23][CH3:24])[CH:8]=1)[CH3:26]

Participants

4

Reactant 3

HCID 2723922Sodium ethoxideHCID 10942334Sodium MethoxideHCID 19348523HCID 19348523, compound

Product 1

HCID 19348676HCID 19348676, compound

Procedure

Following a similar procedure to that described in Preparation 50A, but using an ethanolic sodium ethoxide solution instead of a methanolic sodium methoxide solution, the title compound was obtained as an oily substance.

Sources & evidence

ORD record
ord-167a20cab43644f8910a488041fd2b2e
Source dataset
uspto-grants-2000_03
Patent number
US06040339

Reaction notes

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