HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → HCID 18799400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | (4-Chloropyridin-2-yl)methanol | HCID 2763167 | — |
| Reactant | 3-(Methylamino)-1-propanol | HCID 10148986 | — |
| Product | HCID 18799400 | HCID 18799400 | — |
Reaction Steps
As described in example D3., the title compound is prepared in two steps starting from (4-chloro-pyridin-2-yl)-methanol (15.3 g, 106 mmol) and 3-methylamino-propanol (10.0 g, 112 mmol) and subsequent chlorination of the crude product with N-chlorosuccinimide (19 g, 143 mmol). Yield: 6.4 g (26%), colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043242 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-89abf83d111e48a585d1bdc82a3c9abd |
| Source note | uspto-grants-2000_03 |