HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 492832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 492831 | HCID 492831 | — |
| Reactant | HCID 18799741 | HCID 18799741 | — |
| Product | HCID 492832 | HCID 492832 | — |
Reaction Steps
Following the procedure for the preparation of 4-amino-6-chloro-2-(1-(2-pyridyl)ethyl)thio-pyrimidine but employing an additional alkylation of 4,6-di-(tert-butyldimethylsilyloxy)-2-(1-(2-pyridyl)ethyl)thio-pyrimidine with methyl iodide, this compound is prepared. Melting Pt. 183-184.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043248 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-8fdd653a33d24087a74e6654bf1218d3 |
| Source note | uspto-grants-2000_03 |