HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tryptamine → HCID 5150055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tryptamine | HCID 1150 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 3-Fluoro-p-anisaldehyde | HCID 67696 | — |
| Product | HCID 5150055 | HCID 5150055 | 59% |
Reaction Steps
This product was prepared using the same procedure as for Intermediate 1 with tryptamine (4.80 g, 30.0 mmol), 3-fluoro-4-methoxybenzaldehyde (4.86 g, 1.05 equiv.) and TFA (4.6 mL, 2 equiv.) to give the title compound (5.2 g, 59%) as white crystals. MP: 68° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043252 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-e8267aa8ed3c40a3b7421555fe237326 |
| Source note | uspto-grants-2000_03 |