HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromoaniline → HCID 178517246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromoaniline | HCID 7807 | — |
| Reactant | 1-Acetyl-3-{1-ethoxy-1-phenylmethylidene}-5-nitro-2-indolinone | HCID 54280104 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178517246 | HCID 178517246 | — |
Reaction Steps
Prepared by reacting 1-acetyl-3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone with 1.5 equivalents of 4-bromo-aniline in DMF (110° C., for 2 hours), subsequent treatment with piperidine (20° C., 0.5 hours) and precipitation with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043254 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-3c70e8a8a84848839e3c65f35dae0f8d |
| Source note | uspto-grants-2000_03 |