HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylvaleric acid → HCID 178442264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylvaleric acid | HCID 7341 | — |
| Reactant | 1,4-Naphthalenedione, 2-(acetyloxy)- | HCID 74513 | — |
| Product | HCID 178442264 | HCID 178442264 | 43.4% |
Reaction Steps
The method of Example 1 was followed using 2-acetyloxynaphthalene-1,4-dione (1.24 g, 5.74 mmol) and 2-methylpentanoic acid (1.00 g) yielded the title compound (608 mg) after hydrolysis in. 30 ml THF using potassium hydroxide (5×exess) in water (8 ml) (mp 82-83° C.). This compound is listed as compound 3 in the Tables below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06043286 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-b357fdd3862349cf8d4482da8c07d957 |
| Source note | uspto-grants-2000_03 |