Ethanolamine → HCID 178511457, compound

Participants

Reaction Steps

To a suspension of 2-(2-furyl)-N-(1H-tetrazole-5-yl)-4-thiazolecarboxamide (100 mg) in dry methanol (10 ml) was added 2 -aminoethanol (0.025 ml) and allowed to react, after dissolving, at room temperature for 30 minutes. Then the solvent was removed from the reaction mixture and the residue was crystallized by triturating with dry ether. The produced crystals were filtered with suction and dried to give yellow solids of 2-(2-furyl)-N-(1H-tetrazole-5-yl)-4-thiazolecarboxamide 2-aminoethanol salt (100.3 mg, 81%), m.p. 255°-260° C.

Provenance & Evidence