HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 131716190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 131716191 | HCID 131716191 | — |
| Product | HCID 131716190 | HCID 131716190 | — |
Reaction Steps
Fmoc-Asp(OtBu)-2-(4-methoxyphenyl)ethyl amide (5.44 g; 10 mmoles) was treated with 50% TFA/CH2Cl2 for 90 minutes at room temperature. The solvent was evaporated and the residue was triturated with ethyl ether/petroleum ether. The precipitate was dried and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04879313 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-464d49348f1a43b288edbbe2618256e8 |
| Source note | uspto-grants-1989_11 |