Hexane → HCID 13339543, compound

HRID 1638477Notes

Reaction equation

HRID 1638477 reaction equation
CCCCCC.[Cl:7][C:8]1[CH:9]=[C:10]([N:16]2[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[CH:18]=[CH:17]2)[CH:11]=[CH:12][C:13]=1[O:14][CH3:15].C(OCC)(=[O:27])C>>[Cl:7][C:8]1[CH:9]=[C:10]([N:16]2[C:24]3[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=3)[CH2:18][C:17]2=[O:27])[CH:11]=[CH:12][C:13]=1[O:14][CH3:15]

Participants

4

Reactant 3

HCID 8058HexaneHCID 8857Ethyl AcetateHCID 13339550HCID 13339550, compound

Product 1

HCID 13339543HCID 13339543, compound

Procedure

Using 3:2 hexane:ethyl acetate as eluant on chromatography, the procedure of the preceding preparation was used to convert 1-(3-chloro-4-methoxyphenyl)indole (0.93 g) to present title product, 0.71 g, m.p. 165°-167°.

Sources & evidence

ORD record
ord-c717d18fddde4b9b8a9a37204bced0d8
Source dataset
uspto-grants-1989_11
Patent number
US04879391

Reaction notes

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