HCID 86743501, compound → HCID 18635749, compound

Participants

Reaction Steps

A solution of Compound D (6.76 g) in benzylamine (10 ml) was heated to 120° for 10 minutes. The warm (85°) solution was poured into stirred, distilled water (300 ml) at room temperature. An oil deposited which quickly solidified. After 1 hour's brisk stirring, the buff coloured particulate solid was collected, washed with water and dried to give the title compound 5.03 g, m.pt 155°-165°.

Provenance & Evidence