HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanecarboxylic acid → HCID 22564104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanecarboxylic acid | HCID 7413 | — |
| Reactant | Cyclohexanemethanol | HCID 7507 | — |
| Catalyst | TIN OXIDE (SnO) | HCID 88989 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 22564104 | HCID 22564104 | — |
Reaction Steps
The reaction between cyclohexane carboxylic acid and isopropanol was conducted under the same conditions as in Example 1, except that 1 g of hydrous tin oxide catalyst prepared in Example C was used in place of 2 g of the hydrous zirconium oxide catalyst used in Example 1. It was discovered by gas chromatography that cyclohexyl methanol was formed at a conversion rate of 95% and selectivity of 39%. Isopropyl cyclohexane carboxylic acid was also obtained as a by-product in an amount of 41%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04880937 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-269bf9d0e15d4ae9872659bfd28933c8 |
| Source note | uspto-grants-1989_11 |