HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzenesulfonyl chloride → HCID 14516525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzenesulfonyl chloride | HCID 76187 | — |
| Reactant | 2-Amino-5,7-dimethyl-1,8-naphthyridine | HCID 97365 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 14516525 | HCID 14516525 | — |
Reaction Steps
At an internal temperature of 40° to 50° C., 7.5 g (35.5 mmol) of 2-chlorobenzenesulfonyl chloride was slowly dripped, while stirring, into a suspension of 4.1 g (23.6 mmol) of commercially available 2-amino-5,7-dimethyl-1,8-naphthyridine in 100 ml of anhydrous pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04881969 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-ce018868c05a4f729d1e8776046cb5d5 |
| Source note | uspto-grants-1989_11 |