HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl formate → HCID 70395556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl formate | HCID 7865 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 54296671 | HCID 54296671 | — |
| Product | HCID 70395556 | HCID 70395556 | — |
Reaction Steps
By a procedure analogous to that described in Example 1, part of the crude N-(o-chlorocinnamoyl)sarcosine methyl ester (6.99 g), methyl formate (30 ml) and sodium hydride (2.35 g) gave methyl N-(o-chlorocinnamoyl)-N-methyl-2-amino-3-hydroxypropenoate (4.56 g) as an off-white solid, m.p. 129°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04882341 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-168b6f0f9a984f0cbca9a29f0f0cd290 |
| Source note | uspto-grants-1989_11 |