HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinimide → HCID 15696557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinimide | HCID 11439 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Boron | HCID 5462311 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 15696557 | HCID 15696557 | 66% |
Reaction Steps
The operation is done as for preparation 2, replacing the isopropanol by n-butanol and employing 14.32 g of succinimide in 600 cm3 of n-butanol and 8 g of boron and sodium hydride. 7.5 g of the expected product is obtained, m.p. 36°-38° C. The product can also be prepared by anodic alkylation according to a process described in Synthesis 4, 315-317 (1980).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04882350 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-f9749f3040fb4c8fa82f4ca0208a0db7 |
| Source note | uspto-grants-1989_11 |