참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Hexanol | HCID 8103 | — |
| 반응물 | 5-Hydroxy-2-pyrrolidone | HCID 194148 | — |
| 생성물 | 5-(n-Hexyloxy)-pyrrolidin-2-one | HCID 15696563 | — |
반응 단계
A mixture of 0.4 g of 5-hydroxy-pyrrolidin-2-one, 10 cm3 of n-hexanol and 0.2 g of Amberlite IR 120H is heated to 60° C. for 3 hours. The solvent is distilled off at 25° C. under 0.3 mbar. The residue is chromatographed on silica (eluent: ethyl acetate); 0.5 g of the residue is crystallized from hexane, and the expected product is obtained, m.p. 35°-37° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04882350 |
|---|
| 출처 데이터셋 | uspto-grants-1989_11 |
|---|
| ORD ID | ord-311bf308e5814242ada371960acacaa2 |
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| 출처 메모 | uspto-grants-1989_11 |
|---|
