Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Heptanol | HCID 8129 | — |
| Reactant | 5-Hydroxy-2-pyrrolidone | HCID 194148 | — |
| Product | 5-(n-Heptyloxy)-pyrrolidin-2-one | HCID 15696564 | — |
Reaction Steps
A mixture of 8 g of 5-hydroxy-pyrrolidin-2-one, 100 cm3 of n-heptanol and 4 g of Amberlite IR 120H is heated to 60° C. for 4 hours, filtered, then the solvent is eliminated under 0.3 mbar at 45° C./60° C. 11.9 g of the expected product is obtained, m.p. 52°-54° C., crystallized from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04882350 |
|---|
| Source dataset | uspto-grants-1989_11 |
|---|
| ORD ID | ord-f5ce86bcbe26430bb9df71d5e24a01fe |
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| Source note | uspto-grants-1989_11 |
|---|
