HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-Chloro-1-(4-chloro-2-methylphenoxy)-2-butanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-Chloro-2-methylphenol | HCID 14855 | — |
| Reactant | 1,4-Dichloro-2-butanol | HCID 17021 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | 4-Chloro-1-(4-chloro-2-methylphenoxy)-2-butanol | HCID 13120346 | — |
Reaction Steps
4-Chloro-1(4-chloro-2-methylphenoxy)-2-butanol was prepared according to the procedure of Preparation 4 using 105 g (0.74 mole) of 2-methyl-4-chlorophenol, 171.5 g (1.2 mole) of 1,4-dichloro-2-butanol, 50.3 g of sodium hydroxide, 300 ml of water and 300 ml of tertiary butanol. There was obtained 84 g (45.5%) of product which distilled at 135° C./0.01 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04882330 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-c789af98f46a43a09a400769663f3d53 |
| Source note | uspto-grants-1989_11 |