4-Cyanophenol → HCID 14422834, compound

HRID 1639064Notes

Reaction equation

HRID 1639064 reaction equation
Cl[CH2:2][CH:3]([OH:7])[CH2:4][CH2:5][Cl:6].[C:8]([C:10]1[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=1)#[N:9]>>[Cl:6][CH2:5][CH2:4][CH:3]([OH:7])[CH2:2][O:16][C:13]1[CH:14]=[CH:15][C:10]([C:8]#[N:9])=[CH:11][CH:12]=1

Participants

3

Reactant 2

HCID 130194-CyanophenolHCID 170211,4-Dichloro-2-butanol

Product 1

HCID 14422834HCID 14422834, compoundYield 13%

Procedure

Utilizing the procedure of Preparation 16, 1,4-dichloro-2-butanol was reacted with 4-cyanophenol to give white title compound, m.p. 78°-80° C. in 13% yield.

Sources & evidence

ORD record
ord-631be7b68b0e485ab132fa4ea3fa1c16
Source dataset
uspto-grants-1989_11
Patent number
US04882330

Reaction notes

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