1,4-Dichloro-2-butanol → HCID 14422836, compound

HRID 1639066Notes

Reaction equation

HRID 1639066 reaction equation
Cl[CH2:2][CH:3]([OH:7])[CH2:4][CH2:5][Cl:6].[OH:8][C:9]1[CH:17]=[CH:16][C:12]([C:13]([NH2:15])=[O:14])=[CH:11][CH:10]=1>>[Cl:6][CH2:5][CH2:4][CH:3]([OH:7])[CH2:2][O:8][C:9]1[CH:17]=[CH:16][C:12]([C:13]([NH2:15])=[O:14])=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 170211,4-Dichloro-2-butanolHCID 650524-Hydroxybenzamide

Product 1

HCID 14422836HCID 14422836, compoundYield 25%

Procedure

Utilizing the procedure of Preparation 16, 1,4-dichloro-2-butanol was reacted with 4-hydroxybenzamide to give white title compound, m.p. 150°-153° C. in 25% yield. The recrystallizing solvent was 95% ethanol.

Sources & evidence

ORD record
ord-b03b43f42933475f997b58bf3935f1bd
Source dataset
uspto-grants-1989_11
Patent number
US04882330

Reaction notes

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