HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3078928, compound → HCID 23714429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3078928 | HCID 3078928 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23714429 | HCID 23714429 | — |
Reaction Steps
Compound 1b, 3.3 g, obtained in Example 21 was suspended in 100 ml of methanol and sodium methoxide was added to the solution followed by stirring for about an hour. The solvent was distilled off under reduced pressure and the resulting crude product was solidified by isopropyl ether to give 2.3 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04882351 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-59eec6216fd14c5683f428212082a109 |
| Source note | uspto-grants-1989_11 |