HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorodimethylsilane → [3-(4-Fluoro-3-phenoxyphenyl)propyl]dimethylchlorosilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorodimethylsilane | HCID 66108 | — |
| Reactant | 3-(4-Fluoro-3-phenoxyphenyl)-1-propene | HCID 11075159 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | [3-(4-Fluoro-3-phenoxyphenyl)propyl]dimethylchlorosilane | HCID 19838762 | — |
Reaction Steps
To a stirred mixture of 4.1 g (0.018 mole) of 3-(4-fluoro-3-phenoxyphenyl)-1-propene and 0.060 g (0.00015 mole) of hydrogen hexachloroplatinate hydrate in 15 mL of tetrahydrofuran was added slowly 2.0 g (0.021 mole) of dimethylchlorosilane. Upon completion of addition the reaction mixture was stirred overnight and then was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04883789 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-078dd62b065f4b728382d3b0ce0e7ad8 |
| Source note | uspto-grants-1989_11 |