HRID1639238

反应详情

EQUATION

反应方程式

HRID 1639238 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a stirred mixture of 4.1 g (0.018 mole) of 3-(4-fluoro-3-phenoxyphenyl)-1-propene and 0.060 g (0.00015 mole) of hydrogen hexachloroplatinate hydrate in 15 mL of tetrahydrofuran was added slowly 2.0 g (0.021 mole) of dimethylchlorosilane. Upon completion of addition the reaction mixture was stirred overnight and then was used without further purification.

WORKUP

后处理

  1. additionUpon completion of addition the reaction mixture
  2. customwas used without further purification