HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 19791550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | HCID 19833158 | HCID 19833158 | — |
| Product | HCID 19791550 | HCID 19791550 | — |
Reaction Steps
A melt of 10.1 g (0.038 mol) of 1-(6,7-dichloro-3,4-dihydro-2-naphthyl)pyrrolidine, 5.36 g (0.075 mol) of acrylamide and 0.3 g of p-toluenesulfonic acid is stirred under nitrogen at 100° for 2 hours and at 150° for 2 hours. Recrystallization of the melt cake from ethanol yields 8,9-dichloro-1,4,5,6-tetrahydrobenzo[f]quinolin-3(2H)-one with melting point 260°-261°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04883815 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-08c33cea2a9b40ce99c3bd7eeca379fb |
| Source note | uspto-grants-1989_11 |