HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 1787923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Benzenepropanoyl chloride | HCID 64801 | — |
| Reactant | Methyl carbazate | HCID 80519 | — |
| Product | HCID 1787923 | HCID 1787923 | 80.7% |
Reaction Steps
To a solution of 18 g. (0.2 moles) of methyl carbazate and 100 ml. of acetonitrile 33.7 g (0.2 moles) of β-phenylpropionyl chloride are added dropwise. The reaction mixture is heated to boiling for 15 hours, clarified and cooled. The crystals are filtered off. Thus 36.85 g of the desired compound are obtained, yield 80.7% m.p.: 118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04883907 |
| Source dataset | uspto-grants-1989_11 |
| ORD ID | ord-fa1540cf39b94328a79b5ec674c486ca |
| Source note | uspto-grants-1989_11 |