HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66722410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 66722471 | HCID 66722471 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 66722410 | HCID 66722410 | — |
Reaction Steps
Hydrogen chloride (4.0 M in 1,4-dioxane, 2.0 mL) was added to a solution of tert-butyl (5S)-2-(2-chlorophenyl)-1-oxo-2,7-diazaspiro[4.5]decane-7-carboxylate (0.103 g, 0.000283 mol) in ethyl acetate (0.5 mL) and the mixture was stirred for 2 h. Then the solvent was removed in-vacuo to afford the desired product. LC-MS: 265.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08110581B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-de83ba5bb9284f17a152319c7276d616 |
| Source note | uspto-grants-2012_02 |