反应详情

0.79 g (3.5 mmol) ethyl 2,3-dihydro-1H-indole-3-carboxylate were added batchwise at RT to 7.8 mL (7.8 mmol) of a 1 molar lithium aluminium hydride-THF solution in 40 mL THF and the mixture was refluxed for 1 h. Then the reaction mixture was decomposed with water, while cooling, the precipitate formed was filtered off and the filtrate was evaporated down.

1. temperaturethe mixture was refluxed for 1 h
2. temperaturewhile cooling
3. customthe precipitate formed
4. filtrationwas filtered off
5. customthe filtrate was evaporated down