HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → Diethylether ethylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | Ethylacetate methanol | HCID 21584119 | — |
| Product | Diethylether ethylacetate | HCID 21584169 | 13% |
Reaction Steps
Intermediate 111.i (0.08 g, 0.35 mmol) and intermediate 4.v (0.097 g, 1 eq.) were coupled according to method J. The title compound was isolated after FC (EA/MeOH 9:1+1% NH4OH) and crystallization from EA/ether as a colourless solid (0.022 g, 13% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08114867B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-e54b40fcceb74a71b967b14382ef11a9 |
| Source note | uspto-grants-2012_02 |