HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66738037, compound → HCID 86641876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66738037 | HCID 66738037 | — |
| Reactant | 5-(1-Azidoethyl)-2-fluoropyridine | HCID 86640492 | — |
| Product | HCID 86641876 | HCID 86641876 | — |
Reaction Steps
Using a procedure similar to the one used for 5-(1-azido-ethyl)-2-fluoro-pyridine above, prepare the title intermediate from 1-(4-(benzo[b]thiophen-7-yl)pyridin-3-yl)ethanol as a brown oil (0.66 g, 93%). MS (ES) m/z 280 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08114872B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-094fe00a18fb420db701739b9aed1970 |
| Source note | uspto-grants-2012_02 |